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855016 Rink Amide PEGA resin

Novabiochem®

Rink Amide PEGA resin MSDS (material safety data sheet) or SDS, CoA and CoQ, dossiers, brochures and other available documents.
CAS #: 58318-77-7
855016
Purchase on Sigma-Aldrich

Overview

Replacement Information

Key Spec Table

CAS #
58318-77-7

Products

Catalogue NumberPackaging Qty/Pack
8550160001 Glass bottle 1 g
8550160005 Glass bottle 5 g
8550169999 0
Description
Catalogue Number855016
Replaces01-64-0101
Brand Family Novabiochem®
Background InformationAn excellent acid-labile support for the solid phase synthesis of peptide amides. This resin is prepared by derivatization of amino PEGA resin with the modified Rink linker. It is supplied without Fmoc protection of the linker benzhydrylamine group as this has been found to improve stability. Cleavage is effected with 95% TFA.

PEGA-based resins are compatible with aqueous and alcoholic solvents, and are permeable to macromolecules up to 35 kD.

For further information, please refer to the product entry for amino PEGA resin (855015).

Note: PEGA resins are supplied swollen in ethanol, with 1g dry resin corresponding to approximately 15 mL of swollen resin. As the beads of PEGA resins become very sticky and easily damaged when shrunk or dried, they are best handled in a swollen state. To use, the appropriate amount of swollen resin should be weighed into a reaction vessel and any residual ethanol removed by copious washings with the appropriate solvent or solvent mixture. After peptide assembly, the resin should be washed with DCM and transferred to the cleavage vessel. Excess DCM can be removed under vacuum, and the shrunk resin treated with the TFA cocktail.

The characteristics of the swollen resin, its robustness and high permeability enables its use in both batch and continuous flow synthesis apparatus.

The product number for this product was previously 01-64-0101.

To obtain a certificate of analysis (CoA) of a lot that begins with the letter "A", please select the option in the right hand menu "Request a COA for Lot#s starting with A".
References
Product Information
CAS number58318-77-7
HS Code3907 29 90
Structure formula ImageStructure formula Image
Quality LevelMQ200
Applications
Biological Information
Physicochemical Information
Dimensions
Materials Information
Toxicological Information
Safety Information according to GHS
Storage class10 - 13 Other liquids and solids
WGKWGK 1 slightly hazardous to water
Safety Information
Product Usage Statements
Storage and Shipping Information
StorageStore at +2°C to +8°C.
Packaging Information
Transport Information
Supplemental Information
Specifications
Color (visual)white to yellow to beige
Appearance of substance (visual)beads
Loading (determined from the substitution of the Fmoc-Leu loaded resin)0.20 - 0.50 mmol/g
Swelling Volume (in DMF)lot specific result
dry resin %lot specific result
The resin is sold swollen ethanol.
Global Trade Item Number
Catalogue Number GTIN
8550160001 04027269109837
8550160005 04027269109844
8550169999 04027269109851